Investigation of the elastic properties of cement stone as a factor in ensuring well annular sealing integrity
Mykola Seniushkovych1, Volodymyr Tyrlych1, Oleh Martsynkiv1, Ivan Vytvytskyi1, Ivan Dudych1, Bohdan Martsynkiv1, Ivan Vytvytskyi (Jr.)1
1Ivano-Frankivsk National Technical University of Oil and Gas, Ivano-Frankivsk, Ukraine
Min. miner. depos. 2026, 20(3): 97-107
https://doi.org/10.33271/mining20.03.097
Full text (PDF)
      ABSTRACT
      Purpose. To establish the relationships between the elastic-strength and deformation properties of cement stone and its formation conditions, which determine the integrity and sealing capacity of the cement sheath in oil and gas wells.
      Methods. The research methodology is based on a comprehensive, structured interpretation of experimental datasets cha-racterizing the formation of cement stone produced from the base PCT I-100 Portland well cement. The relationships between the elastic and mechanical properties of the cement stone were evaluated using correlation analysis. Regression analysis incorporating the full set of available explanatory variables was used to develop mathematical models describing changes in cement stone properties under different formation conditions.
      Findings. Young’s modulus, strength, and deformation characteristics of cement stone depend substantially on curing age and temperature. A high curing temperature (75°C) accelerates the early development of elastic and strength properties and reduces creep deformation, but it does not yield the highest long-term strength. At 20°C, curing proceeds more slowly; however, at later stages, it results in greater stiffness and a more sustained increase in strength. Creep and residual deformation decrease with age, although their values are considerably higher at lower temperatures, thereby increasing the risk of defects in the wellbore casing system.
      Originality. The importance of determining the elastic properties of cement stone, a key factor in the formation of leakage microchannels in wellbore casing systems, has been demonstrated. It was established that cement stone produced from the base PCT I-100 Portland well cement exhibits insufficient elastic properties at early curing stages, which may result in loss of contact with the casing string and surrounding rock under operational loading. Mathematical regression models were developed to assess the potential risk of leakage pathway formation during the early stages of cement stone curing by integrating the relationships between its mechanical properties and formation conditions.
      Practical implications. The identified patterns in the deformation characteristics of cement stone can be useful for research institutions and industrial enterprises developing cement slurry formulations for well cementing.
      Keywords: well; cementing; portland cement; cement stone; tightness
      REFERENCES
- Guo, S., Bu, Y., Yang, X., Wang, C., Guo, B., & Sun, B. (2020). Effect of casing internal pressure on integrity of cement ring in marine shallow formation based on XFEM. Engineering Failure Analysis, 108, 104258. https://doi.org/10.1016/j.engfailanal.2019.104258
- Li, M., Zhou, F., Wang, B., Hu, X., Wang, D., & Zhuang, X. (2022). Numerical simulation on the multiple planar fracture propagation with perforation plugging in horizontal wells. Petroleum Science, 19(5), 2253-2267. https://doi.org/10.1016/j.petsci.2022.05.004
- Alkhamis, M., & Imqam, A. (2018). New cement formulations utilizing graphene nano platelets to improve cement properties and long-term reliability in oil wells. SPE Kingdom of Saudi Arabia Annual Technical Symposium and Exhibition, SPE-192342-MS. https://doi.org/10.2118/192342-ms
- Vytvytskyi, I.I., Seniushkovych, M.V., & Shatskyi, I.P. (2017). Calculation of distance between elastic-rigid centralizers of casing. Naukovyi Visnyk Natsionalnoho Hirnychoho Universytetu, 5, 29-35.
- Shatskyi, I., Vytvytskyi, I., Senyushkovych, M., & Velychkovych, A. (2019). Modelling and improvement of the design of hinged centralizer for casing. IOP Conference Series: Materials Science and Engineering, 564(1), 012073). https://doi.org/10.1088/1757-899X/564/1/012073
- Shatskyi, I., Velychkovych, A., Vytvytskyi, I., & Seniushkovych, M. (2019). Analytical models of contact interaction of casing centralizers with well wall. Engineering Solid Mechanics, 7, 355-366. https://doi.org/10.5267/j.esm.2019.6.002
- Moradi, S.S.T., & Nikolaev, N. (2016). Considerations of well cementing materials in high-pressure, high-temperature conditions (Research note). International Journal of Engineering, 29(9), 1214-1218.
- Ahdaya, M., & Imqam, A. (2019). Investigating geopolymer cement performance in presence of water based drilling fluid. Journal
- Bois, A.P., Garnier, A., Rodot, F., Sain-Marc, J., & Aimard, N. (2011). How to prevent loss of zonal isolation through a comprehensive analysis of microannulus formation. SPE Drilling & Completion, 26(01),
- Bois, A.-P., Garnier, A., Galdiolo, G., & Laudet, J.B. (2012). Use of a Mechanistic Model To Forecast Cement-Sheath Integrity. SPE Drilling & Completion, 27(02), 303-314. https://doi.org/10.2118/139668-pa
- Skadsem, H.J. (2022). Characterization of annular cement permeability of a logged well section using pressure-pulse decay measurements. Journal of Energy Resources Technology, 144(5), JERT-21-1810. https://doi.org/10.1115/1.4053709
- Castel, A., & Foster, S.J. (2015). Bond strength between blended
- Nalyvaiko, O.I., Romashko, O.V., & Kaptsova, N.I. (2020). Laboratorno-vyrobnychi doslidzhennia vlastyvosti tamponazh-noho kameniu. Voda. Ekolohiia. Suspilstvo.
- Jackson, P.B., & Murphey, C.E. (1993). Effect of casing pressure on gas flow through a sheath of set cement. Proceedings of the SPE/IADC Drilling Conference, SPE-25698-MS. https://doi.org/10.2118/25698-ms
- Thiercelin, M.J., Dargaud, B., Baret, J.F., & Rodriguez, W.J. (1997). Cement design based on cement mechanical response. SPE Annual Technical Conference and Exhibition. https://doi.org/10.2118/38598-ms
- Parcevaux, P.A., & Sault, P.H. (1984). Cement shrinkage and elasticity: A new approach for a good zonal isolation. SPE Annual Technical Conference and Exhibition, SPE-13176-MS. https://doi.org/10.2118/13176-ms
- Jensen, O.M., & Hansen, P.F. (2001). Autogenous deformation and RH-change in perspective. Cement and Concrete Research, 31(12), 1859-1865. https://doi.org/10.1016/s0008-8846(01)00501-4
- Reddy, B.R., Xu, Y., Ravi, K., Gray, D. W., & Pattillo, P. (2009). Cement shrinkage measurement in oilwell cementing-a comparative study of laboratory methods and procedures. SPE Drilling & Completion, 24(01), 104-114. https://doi.org/10.2118/103610-pa
- Abuhaikal, M., Musso, S., Thomas, J., & Ulm, F.J. (2013). An apparatus for dissecting volumetric changes in hydrating cement paste. Proceedings of the Ninth International Conference on Creep, Shrinkage, and Durability Mechanics. https://doi.org/10.1061/9780784413111.037
- Lima, V.N., Silva, F.d.A., Skadsem, H.J., Beltrán-Jiménez, K., & Sunde, J.K. (2022). Effects of confinement pressure on the mechanical behavior of an oil well cement paste. Journal of Petroleum Science and Engineering, 208, 109769. https://doi.org/10.1016/j.petrol.2021.109769
- Song, J., Xu, M., Tan, C., You, F., Wang, X., & Zhou, S. (2022). Study on an epoxy resin system used to improve the elasticity of oil-well cement-based composites. Materials, 15(15), 5258. https://doi.org/10.3390/ma15155258
- Sudong, H., & Xiao, Y. (2007). Properties and application of oil-well cement enhanced with a novel composite toughening agent. Petroleum Science, 4(2), 52-59. https://doi.org/10.1007/bf03187442
- Moghadam, A., Castelein, K., ter Heege, J., & Orlic, B. (2021). A study on the hydraulic aperture of microannuli at the casing-cement interface using a large-scale laboratory setup. Geomechanics for Energy and the Environment, 100269. https://doi.org/10.1016/j.gete.2021.100269
- Astakhova, N. V. (2022). Doslidzhennia deformatyvnykh vlastyvostei tsementnoho kameniu z vykorystanniam aktyvovanykh vidkhodiv HZK. Visnyk Kryvorizkoho Natsionalnoho Universytetu, 54, 98-103. https://doi.org/10.31721/2306-5451-2022-1-54-98-103
- Kaminskyi, A.T. (2021). Remontni sumishi z pidvyshchenymy ekspluatatsiinymy vlastyvostiamy na osnovi luzhnoho portlandtsementu. Dysertatsiia na zdobuttia naukovoho stupenia doktora filosofii. Lviv, Ukraina: Natsionalnyi universytet “Lvivska politekhnika”.
- He, M., Song, J., Xu, M., He, L., & Xu, P. (2020). Effect of epoxy resin emulsion on the mechanical properties of oil well cement-based composites. Advances in Civil Engineering, 2020, 1-9. https://doi.org/10.1155/2020/5344866
- Yakovleva, A.A., Movchan, I.B., & Shaygallyamova, Z.I. (2022). Dynamic response of multi-scale geophysical systems: waves and practical applications. Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, 380(2237), 20210403. https://doi.org/10.1098/rsta.2021.0403
- Hlukhovskyi, V.V., & Hlukhovskyi, I.V. (2024). Udaromitsni dyspersno-armovani kompozyty na osnovi neorhanichnykh viazhuchykh ta mineralnykh volokon. Vcheni zapysky TNU imeni V.I. Vernadskoho. Seriia: Tekhnichni nauky, 35(74(2)), 240-245. https://doi.org/10.32782/2663-5941/2024.2/32
- Jutten, J.J., & Hayman, A.J. (1993). Microannulus effect on cementation logs: experiments and case histories. SPE Asia Pacific Oil and Gas Conference, SPE-25377-MS. https://doi.org/10.2118/25377-ms
- Liashenko, A.V., Zaliskyi, O.V., & Chernushenko, M.I. (2024). Vykorystannia tsementno-polimernykh materialiv dlia kriplennia sverdlovyn. Zbirnyk XVII Mizhnarodnoi Naukovo-Praktychnoi Konferentsii “Akademichna Universytetska Nauka: Rezultaty ta Perspektyvy. Sektsiia “Vyrobnytstvo, Tekhnolohii, Inzheneriia”, 380-382.
- Nemakh, A., Nesterenko, S., Donskyi, D., & Skrypii, Yu. (2020). Doslidzhennia dynamiky sirkovodnevoi korozii metalu obsadnoi kolony pid sharom modyfikovanoho betonu. Komunalne Hospodarstvo Mist, 3(156), 49-55. https://doi.org/10.33042/2522-1809-2020-3-156-49-55
- Jennings, S.S. (2005). Long-term high-temperature laboratory cement data aid in the selection of optimized cements SPE-95816-MS. SPE Annual Technical Conference and Exhibition. https://doi.org/10.2118/95816-ms
- Anya, A., Emadi, H., & Watson, M. (2020). Effect of size and shape of oil well cement test specimen on uniaxial compressive strength measurements. Journal of Petroleum Science and Engineering, 195, 107538. https://doi.org/10.1016/j.petrol.2020.107538
- DSTU B V.2.7-88-99. (1999). Portlandtsementy tamponazhni.
- DSTU B V.2.7-217:2009. (2009). Metody vyznachennia pryzmovoi mitsnosti, modulia pruzhnosti i koefitsiienta Puassona.
- ASTM D2990-17. (2025). Standard test methods for tensile, compressive, and flexural creep and creep-rupture of plastics.
- ISO 899-1:2017. (2017). Plastics – Determination of creep behaviour. Part 1: Tensile creep.
- Bewick, V., Cheek, L., & Ball, J. (2003). Critical Care, 7(6), 451. https://doi.org/10.1186/cc2401
- de Winter, J.C.F., Gosling, S.D., & Potter, J. (2016). Comparing the Pearson and Spearman correlation coefficients across distributions and sample sizes: A tutorial using simulations and empirical data. Psychological Methods, 21(3), 273-290. https://doi.org/10.1037/met0000079
- Tibshirani, R. (1996). Regression shrinkage and selection via the lasso. Journal of the Royal Statistical Society: Series B (Methodological), 58(1), 267-288. https://doi.org/10.1111/j.2517-6161.1996.tb02080.x
- Heinze, G., Wallisch, C., & Dunkler, D. (2018). Variable selection – A review and recommendations for the practicing statistician. Biometrical Journal, 60(3), 431-449. https://doi.org/10.1002/bimj.201700067
- Luijken, K., Groenwold, R.H.H., van Smeden, M., Strohmaier, S., & Heinze, G. (2022). A comparison of full model specification and backward elimination of potential confounders when estimating marginal and conditional causal effects on binary outcomes from observational data. Biometrical Journal. https://doi.org/10.1002/bimj.202100237
- Zou, H., & Hastie, T. (2005). Regularization and variable selection via the elastic net. Journal of the Royal Statistical Society: Series B (Statistical Methodology), 67(2), 301-320. https://doi.org/10.1111/j.1467-9868.2005.00503.x
- Chicco, D., Warrens, M.J., & Jurman, G. (2021). The coefficient of determination R-squared is more informative than SMAPE, MAE, MAPE, MSE and RMSE in regression analysis evaluation. PeerJ Computer Science, 7, e623. https://doi.org/10.7717/peerj-cs.623
- Hodson, T.O. (2022). Root-mean-square error (RMSE) or mean absolute error (MAE): When to use them or not. Geoscientific Model Development, 15(14), 5481-5487. https://doi.org/10.5194/gmd-15-5481-2022
- Shatz, I. (2023). Assumption-checking rather than (just) testing: The importance of visualization and effect size in statistical diagnostics. Behavior Research Methods, 56, 826-845. https://doi.org/10.3758/s13428-023-02072-x
- Feng, C., Li, L., & Sadeghpour, A. (2020). A comparison of residual diagnosis tools for diagnosing regression models for count data. BMC Medical Research Methodology, 20(1), 175. https://doi.org/10.1186/s12874-020-01055-2
